Atom Probe Studies on Nanocrystallization of Amorphous Alloys.
نویسندگان
چکیده
منابع مشابه
Atom Probe Studies of Nanocrystallization of Amorphous Alloys
The nanocrystallization processes in Fe-Si-B-Nb-Cu and Fe-Nd-B(-Cu-Nb) amorphous alloys have been studied by transmission electron microscopy (TEM) and a three dimensional atom probe (3DAP). Cu additions are effective in refining the nanocrystalline microstructures of an Fe74.5Si13.5B8Nb3Cu1 alloy and an Fe3B/Nd2Fe14B nanocomposite microstructure. This is because Cu atoms form a high density of...
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Nanocrystals develop in amorphous alloys usually during annealing treatments with growth- or nucleation-controlled mechanisms. An alternative processing route is intense deformation and nanocrystals have been shown to develop in shear bands during the deformation process. Some controversy surrounded the idea of adiabatic heating in shear bands during their genesis, but specific experiments have...
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Crystallization kinetics of Fe52Cr18Mo7B16C4Nb3 alloy was evaluated using X-ray diffraction, differential scanning calorimetric (DSC) tests and TEM observations in this research work. In effect, crystallization and growth mechanisms were investigated using DSC tests in four different heating rates (10, 20, 30, 40 K/min) and kinetic models (i.e. Kissinger- Starink, Ozawa, and Matusita methods). ...
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Pre-precipitation stages of Al-0.70Mg-0.33Si and Al-0.65Mg-0.70Si (at.%) alloys have been investigated by atom probe field ion microscopy (APFIM) and high resolution transmission electron microscopy (HREM). Atom probe results show that clusters of Mg atoms are present in the asquenched state. After a prolonged aging at room temperature, clusters of Mg, Si and their co-clusters are detected, alt...
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Using conventional and high-resolution transmission electron microscopy (HRTEM), the effects of rolling at room temperature on the microstructures of amorphous Al90Fe5Gd5 and Al86.8Ni3.7Y9.5 were compared. In rolled Al90Fe5Gd5, nanocrystallites were observed at shear bands, whereas none were observed in rolled Al86.8Ni3.7Y9.5. When HRTEM was combined with with Fourier transform filtering, nanos...
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ژورنال
عنوان ژورنال: Materia Japan
سال: 1996
ISSN: 1340-2625,1884-5843
DOI: 10.2320/materia.35.843